About acid catalysed acetonation reactions of d-ribose

Capa

Citar

Texto integral

Acesso aberto Acesso aberto
Acesso é fechado Acesso está concedido
Acesso é fechado Acesso é pago ou somente para assinantes

Resumo

For comparative identification of side products of the cyanation reaction of the imidate donor with trimethylsilyl cyanide, the main compounds formed in the acetonation reactions of D-ribose catalyzed by H2SO4, p -TSA, CSA, and PPTS were synthesized and characterized. The structures of the latter were correctly refined by spectral methods using 2D technologies and high-resolution mass spectrometry.

Sobre autores

Z. Valiullina

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

N. Ivanova

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

G. Shavaleeva

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

N. Akhmetdinova

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

A. Lobov

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

M. Abdullin

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

M. Miftakhov

Ufa Institute of Chemistry UFRC RAS

Email: gushavaleeva@mail.ru

Bibliografia

  1. Simeonov S.P., Nunes J.P.M., Guerra K., Kurteva V.B. Chem. Rev. 2016, 116, 5744-5893. doi: 10.1021/cr500504w
  2. Johnson C.R., Chen Y.F. J. Org. Chem. 1991, 56, 3344-3351. doi: 10.1021/jo00010a031
  3. Elhalem E., Comin M.J., Leitofuter J., Garcia-Linares G. Tetrahedron Asymmetry. 2005, 16, 425-431. doi: 10.1016/j.tetasy.2004.11.069
  4. Gallos J.K., Stathakis C.I., Kotoulas S.S., Koumbis E. J. Org. Chem. 2005, 70, 6884-6890. doi: 10.1021/jo050987t
  5. Li B., Wang H., Sun C., Lu S., Kang L., Jiang S. Heterocycles. 2021, 102, 1797-1802. doi: 10.3987/COM-21-14499
  6. Mydock L.K., Demchenko A.V. Org. Biomol. Chem. 2010, 8, 497-510. doi: 10.1039/B916088D
  7. Toshima K. Carbohydr. Res. 2006, 341, 1282-1297. doi: 10.1016/j.carres.2006.03.012
  8. Boons G-J. Tetrahedron. 1996, 52, 1095-1121. doi: 10.1016/0040-4020(95)00897-7
  9. Yang L., Qin Q., Ye X.-S. Asian J. Org. Chem. 2013, 2, 30-49. doi: 10.1002/ajoc.201200136
  10. Winkler T., Ernst B. Helv. Chim. Acta. 1988, 71, 120-123. doi: 10.1002/hlca.19880710114
  11. Vis E., Fletcher Jr. H.G. J. Am. Chem. Soc. 1957, 79, 1182-1185. doi: 10.1021/ja01562a040
  12. Hughes N.A., Speakman P.R.H. Carbohydr. Res. 1965, 1, 176-175. doi: 10.1016/S0008-6215(00)80921-0
  13. Fleetwood A., Hughes N.A. Carbohydr. Res. 1999, 317, 204-209. doi: 10.1016/S0008-6215(99)00064-6

Arquivos suplementares

Arquivos suplementares
Ação
1. JATS XML
Baixar

Declaração de direitos autorais © Russian Academy of Sciences, 2023