Experimental Setup for Synchrotron Studies of Materials under Influence of External Magnetic Fields

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Abstract

A specialized experimental setup has been designed and manufactured for X-ray diffraction studies under the influence of external magnetic fields on the sample. The setup includes a set of precision automated electromechanical drives that enable orientation of the permanent magnet-based magnetic system along various crystallographic directions of the studied sample. The system provides automated variation of the external magnetic field strength and direction during the experiment. The setup is compatible with blow-out type temperature attachments, allowing for research within a wide temperature range. The specified performance characteristics of the setup and its high parameter stability have been validated through a series of experiments with X-ray scattering near absorption edges using iron borate single crystals.

About the authors

N. I. Snegirev

Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”

Email: niksnegir@yandex.ru
Moscow, 119333 Russia

A. G. Kulikov

Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”

Moscow, 119333 Russia

Y. M. Dymshits

Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”

Moscow, 119333 Russia

F. S. Pilyak

Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”

Moscow, 119333 Russia

M. M. Borisov

National Research Center “Kurchatov Institute”

Moscow, 123182 Russia

E. K. Mukhamedzhanov

National Research Center “Kurchatov Institute”

Moscow, 123182 Russia

Y. V. Pisarevsky

Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”

Moscow, 119333 Russia

I. S. Lyubutin

Shubnikov Institute of Crystallography of the Kurchatov Complex Crystallography and Photonics of the NRC “Kurchatov Institute”

Moscow, 119333 Russia

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